Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-12-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0332 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 82.330, 82.330, 134.320 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.890 - 1.420 |
| Rwork | 0.154 |
| R-free | 0.17140 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7jrn |
| RMSD bond length | 0.020 |
| RMSD bond angle | 2.308 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.890 | 1.440 |
| High resolution limit [Å] | 1.420 | 1.420 |
| Number of reflections | 99793 | 4864 |
| <I/σ(I)> | 28.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 52.9 | |
| CC(1/2) | 0.970 | 0.360 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 277 | 1.0M NaH2PO4/1.0MKH2PO4 100mM Tris_HCl pH=7.5 |
