7M0L
HPK1 IN COMPLEX WITH COMPOUND 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0001 |
Spacegroup name | P 1 |
Unit cell lengths | 44.850, 76.723, 88.413 |
Unit cell angles | 89.97, 97.84, 90.03 |
Refinement procedure
Resolution | 87.590 - 2.430 |
R-factor | 0.247 |
Rwork | 0.246 |
R-free | 0.29280 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PREVIOUSLY SOLVED STRUCTURE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.572 |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.590 | 2.680 |
High resolution limit [Å] | 2.430 | 2.430 |
Rmeas | 0.057 | 0.563 |
Number of reflections | 42306 | 10850 |
<I/σ(I)> | 12.89 | 2.99 |
Completeness [%] | 96.1 | 96.2 |
Redundancy | 2.2 | 2.1 |
CC(1/2) | 0.999 | 0.998 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 20 mM Tris pH 8.0 , 150 mM NaCl , 5% Glycerol , 2 mM DTT |