7KJU
Cgi121-tRNA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-21 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97964 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 100.493, 168.527, 68.968 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.034 - 3.102 |
R-factor | 0.2492 |
Rwork | 0.248 |
R-free | 0.26650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3l0u |
Data reduction software | DIALS (1.14.5) |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.16) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.140 | 49.140 | 3.190 |
High resolution limit [Å] | 3.100 | 13.910 | 3.110 |
Rmerge | 0.081 | 0.036 | 0.931 |
Rmeas | 0.085 | 0.038 | 0.989 |
Rpim | 0.025 | 0.012 | 0.330 |
Total number of observations | 1211 | 7016 | |
Number of reflections | 10895 | 127 | 792 |
<I/σ(I)> | 13.3 | 36.8 | 2.1 |
Completeness [%] | 99.9 | 87.2 | 100 |
Redundancy | 11.8 | 9.5 | 8.9 |
CC(1/2) | 0.999 | 0.999 | 0.956 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 100 mM MES, pH 6.0, 0.2 M zinc acetate, 10% PEG8000 |