7JJK
Crystal structure of SOX30
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2020-02-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95372 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 33.770, 35.700, 52.910 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.990 - 1.400 |
R-factor | 0.1749 |
Rwork | 0.174 |
R-free | 0.19920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o4x |
RMSD bond length | 0.009 |
RMSD bond angle | 1.192 |
Data reduction software | Aimless |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.990 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Number of reflections | 13155 | 656 |
<I/σ(I)> | 17.8 | |
Completeness [%] | 99.9 | |
Redundancy | 11.8 | |
CC(1/2) | 0.999 | 0.968 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 296 | 0.1 M sodium acetate pH 4.6, 2 M ammonium sulfate |