7JIU
HUMAN PI3KDELTA IN COMPLEX WITH COMPOUND 2F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-09-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00003 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.457, 135.132, 142.045 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 97.910 - 2.120 |
R-factor | 0.2127 |
Rwork | 0.212 |
R-free | 0.24590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PREVIOUSLY DETERMINED STRUCTURE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.269 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 97.910 | 2.370 |
High resolution limit [Å] | 2.120 | 2.120 |
Rmeas | 0.071 | 0.614 |
Number of reflections | 64620 | 18062 |
<I/σ(I)> | 19.4 | 3.99 |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 8.1 | 8.4 |
CC(1/2) | 0.999 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | NOT AVAILABLE |