7EXC
Crystal structure of T2R-TTL-1129A2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-10 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97777 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 105.248, 157.375, 181.974 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.850 - 2.390 |
R-factor | 0.2193 |
Rwork | 0.218 |
R-free | 0.26350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7cda |
RMSD bond length | 0.009 |
RMSD bond angle | 1.179 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.850 | 2.460 |
High resolution limit [Å] | 2.390 | 2.400 |
Number of reflections | 119090 | 7832 |
<I/σ(I)> | 5.9 | |
Completeness [%] | 100.0 | |
Redundancy | 9.8 | |
CC(1/2) | 0.995 | 0.711 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 6% poly(ethylene glycol) 4000, 8% glycerol, 0.1 M MES (pH 6.7), 30 mM CaCl2, 30 mM MgCl2 |