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7EQ2

Crystal structure of GDP-bound Rab1a-T75D

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U
Synchrotron siteSSRF
BeamlineBL17U
Temperature [K]100
Detector technologyCCD
Collection date2015-12-12
DetectorADSC QUANTUM 315r
Wavelength(s)0.977760
Spacegroup nameP 1
Unit cell lengths39.489, 50.598, 52.626
Unit cell angles76.94, 84.62, 86.27
Refinement procedure
Resolution25.116 - 1.551
R-factor0.161457428126
Rwork0.160
R-free0.18519
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2fol
RMSD bond length0.006
RMSD bond angle0.902
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareMOLREP
Refinement softwarePHENIX (1.11.1_2575)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.1201.610
High resolution limit [Å]1.5511.551
Number of reflections544165434
<I/σ(I)>42.71
Completeness [%]95.2
Redundancy3.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1EVAPORATION291.1540mM Lithium chloride, 20mM Magnesium chloride hexahydrate, 80mM NaCl, 2mM Hexammine cobalt(III) chloride, 40mM Sodium cacodylate trihydrate pH 5.5, 30% v/v (+/-)-2-Methyl-2,4-pentanediol

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