7EPE
Crystal structure of mGlu2 bound to NAM563
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 58.521, 86.402, 99.630 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.144 | |
Number of reflections | 17691 | 1681 |
<I/σ(I)> | 28.1 | |
Completeness [%] | 99.2 | |
Redundancy | 9.3 | |
CC(1/2) | 0.514 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIPIDIC CUBIC PHASE | 293.15 | 100 mM HEPES, pH 7.0, 100~200 mM NaCl, 100~200 mM MgCl2, and 20~30%(v/v) PEG 400 |