7BI9
PI3KC2a core in complex with PIK90
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-17 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9184 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.943, 135.397, 151.603 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.940 - 2.650 |
R-factor | 0.235 |
Rwork | 0.233 |
R-free | 0.27980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7bi4 |
RMSD bond length | 0.002 |
RMSD bond angle | 1.205 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.940 | 2.810 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmeas | 0.125 | 2.129 |
Number of reflections | 33099 | 5274 |
<I/σ(I)> | 11.16 | |
Completeness [%] | 96.2 | 96.3 |
Redundancy | 4 | |
CC(1/2) | 0.998 | 0.380 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 0.1MTris, 8-6% PEG3350, 0.2-0.1M MgSO4 |