7AMK
Zebrafish RET Cadherin Like Domains 1 to 4.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9787 |
Spacegroup name | P 1 |
Unit cell lengths | 51.167, 70.499, 105.438 |
Unit cell angles | 105.41, 100.93, 100.25 |
Refinement procedure
Resolution | 65.960 - 2.200 |
R-factor | 0.2273 |
Rwork | 0.225 |
R-free | 0.26940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x2u |
RMSD bond length | 0.008 |
RMSD bond angle | 0.888 |
Data reduction software | DIALS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (dev_3965) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.960 | 2.190 |
High resolution limit [Å] | 2.080 | 2.080 |
Rmerge | 0.080 | 1.186 |
Rmeas | 0.095 | 1.416 |
Rpim | 0.051 | 0.765 |
Number of reflections | 79868 | 11549 |
<I/σ(I)> | 6.2 | 1.4 |
Completeness [%] | 98.2 | 97.2 |
Redundancy | 3.4 | 3.3 |
CC(1/2) | 0.996 | 0.580 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | 50 mM MES (pH 6.2), 31.5 % PEG MME 350 (v/v) |