7VHZ
Crystal structure of EP300 HAT domain in complex with compound 7
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-08 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.100000 |
Spacegroup name | P 1 |
Unit cell lengths | 43.676, 89.219, 91.132 |
Unit cell angles | 114.99, 95.33, 92.02 |
Refinement procedure
Resolution | 19.980 - 2.000 |
R-factor | 0.1924 |
Rwork | 0.191 |
R-free | 0.21880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bhw |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.980 | 19.980 | 2.120 |
High resolution limit [Å] | 2.000 | 5.960 | 2.000 |
Rmerge | 0.044 | 0.021 | 0.577 |
Rmeas | 0.062 | 0.030 | 0.815 |
Total number of observations | 144642 | ||
Number of reflections | 78731 | 2736 | 12456 |
<I/σ(I)> | 10.72 | 34.69 | 1.23 |
Completeness [%] | 94.2 | 86.4 | 92.3 |
Redundancy | 1.837 | 1.819 | 1.779 |
CC(1/2) | 0.998 | 0.999 | 0.564 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 16% PEG3350, 0.1 M HEPES (pH 7.0) |