Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-03-21 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.989, 95.733, 68.579 |
| Unit cell angles | 90.00, 91.98, 90.00 |
Refinement procedure
| Resolution | 47.870 - 1.950 |
| R-factor | 0.2112 |
| Rwork | 0.210 |
| R-free | 0.24190 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2qnj |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.057 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER (v7.1.015) |
| Refinement software | REFMAC (v7.1.015) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.870 | 2.020 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.079 | 0.543 |
| Number of reflections | 47368 | 4760 |
| <I/σ(I)> | 11.8 | 2.47 |
| Completeness [%] | 98.7 | 99.44 |
| Redundancy | 3.5 | 3.6 |
| CC(1/2) | 0.996 | 0.782 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1 M sodium formate pH 7.0 24% PEG3350 |
