Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

7K9Q

Co-crystal structure of alpha glucosidase with compound 4

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-B
Synchrotron siteAPS
Beamline23-ID-B
Temperature [K]100
Detector technologyPIXEL
Collection date2020-04-08
DetectorDECTRIS EIGER X 16M
Wavelength(s)0.9793
Spacegroup nameP 32
Unit cell lengths102.876, 102.876, 241.696
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution42.490 - 2.300
R-factor0.1724
Rwork0.172
R-free0.19740
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5f0e
RMSD bond length0.004
RMSD bond angle0.747
Data reduction softwareHKL-2000 (v717.1)
Data scaling softwareHKL-2000 (v717.1)
Phasing softwarePHENIX
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]42.4902.386
High resolution limit [Å]2.3002.300
Rmerge0.1311.105
Rmeas0.1401.190
Rpim0.0480.437
Number of reflections12635612577
<I/σ(I)>11.3
Completeness [%]99.999.31
Redundancy8.3
CC(1/2)0.9920.608
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP72970.09M NPS, 0.1M Buffer system 1 pH7.0, 29%v/v P500MME_P20K (Morpheus screen, condition C1)

219869

PDB entries from 2024-05-15

PDB statisticsPDBj update infoContact PDBjnumon