6ZTR
Crystal Structure of the anti-human P-Cadherin Fab CQY684 in complex with human P-Cadherin(108-324)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-06-10 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.999990 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 172.691, 77.795, 133.406 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 72.490 | 72.490 | 2.150 |
High resolution limit [Å] | 2.100 | 9.390 | 2.100 |
Rmerge | 0.199 | 0.039 | 2.392 |
Rmeas | 0.216 | 0.043 | 2.585 |
Total number of observations | 707980 | ||
Number of reflections | 105445 | 1337 | 7725 |
<I/σ(I)> | 7.97 | 33.36 | 0.88 |
Completeness [%] | 100.0 | 99.3 | 100 |
Redundancy | 6.714 | 6.073 | 6.967 |
CC(1/2) | 0.995 | 0.995 | 0.396 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.2M calcium acetate, 10% (w/v) PEG 8,000, 0.1M MES pH 6.5 |