6ZHS
Uba1 bound to two E2 (Ubc13) molecules
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-26 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 177.710, 72.900, 139.520 |
Unit cell angles | 90.00, 112.43, 90.00 |
Refinement procedure
Resolution | 24.920 - 2.350 |
R-factor | 0.2188 |
Rwork | 0.216 |
R-free | 0.27490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cmm |
RMSD bond length | 0.003 |
RMSD bond angle | 0.632 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.435 |
High resolution limit [Å] | 2.350 | 2.350 |
Number of reflections | 67708 | 398 |
<I/σ(I)> | 6.97 | |
Completeness [%] | 66.1 | |
Redundancy | 5.6 | |
CC(1/2) | 0.987 | 0.424 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 273 | ammonium sulfate, HEPES, PEG 3350 |