6Z3H
Repulsive Guidance Molecule B (RGMB) in complex with Growth Differentiation Factor 5 (GDF5) (crystal form 2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 98.860, 98.860, 99.810 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.430 - 3.158 |
R-factor | 0.2362 |
Rwork | 0.234 |
R-free | 0.26820 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ui0 |
RMSD bond length | 0.001 |
RMSD bond angle | 0.376 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.15rc3_3435: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.980 | 3.210 |
High resolution limit [Å] | 3.130 | 3.130 |
Rmerge | 0.081 | |
Number of reflections | 5352 | 380 |
<I/σ(I)> | 23.4 | 1.1 |
Completeness [%] | 97.6 | |
Redundancy | 35.8 | |
CC(1/2) | 0.806 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 0.2 M (NH4)2SO4, 0.1 M sodium acetate pH 4.6, 35% w/v pentaerythritol ethoxylate (15/4 EO/OH; average MW 797 Da) |