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6YIF

Structure of Chromosomal Passenger Complex (CPC) bound to phosphorylated Histone 3 peptide at 1.8 A.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I24
Synchrotron siteDiamond
BeamlineI24
Temperature [K]110
Detector technologyPIXEL
Collection date2017-10-21
DetectorDECTRIS PILATUS3 6M
Wavelength(s)0.96859
Spacegroup nameP 65
Unit cell lengths98.863, 98.863, 56.067
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution49.430 - 1.810
R-factor0.1828
Rwork0.181
R-free0.22270
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2qfa
RMSD bond length0.011
RMSD bond angle1.149
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX (1.16_3549)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]49.4301.860
High resolution limit [Å]1.8101.810
Rmerge0.0480.953
Number of reflections284542126
<I/σ(I)>13.81.4
Completeness [%]99.4
Redundancy4.4
CC(1/2)0.9970.544
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION6.529120 % (w/v) PEG 4,000, 200 mM Lithium sulphate, 50 mM MES pH 6.5

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