6W8W
Crystal structure of mouse DNMT1 in complex with CCG DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 89.794, 152.593, 95.631 |
Unit cell angles | 90.00, 94.74, 90.00 |
Refinement procedure
Resolution | 48.440 - 3.000 |
R-factor | 0.2398 |
Rwork | 0.238 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4da4 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.110 |
High resolution limit [Å] | 2.990 | 6.460 | 3.000 |
Rmerge | 0.274 | 0.087 | 1.034 |
Rmeas | 0.302 | 0.094 | 1.162 |
Rpim | 0.123 | 0.036 | 0.517 |
Number of reflections | 50826 | 5192 | 4994 |
<I/σ(I)> | 1.9 | ||
Completeness [%] | 98.2 | 98.3 | 96.8 |
Redundancy | 5.6 | 6.5 | 4.4 |
CC(1/2) | 0.996 | 0.304 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.8 | 277 | 0.1 M Sodium Citrate, 10 mM ZnCl2 |