6VIF
Human LRH-1 ligand-binding domain bound to agonist cpd 15 and fragment of coregulator TIF-2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 46.134, 46.134, 223.436 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.640 - 2.260 |
R-factor | 0.2423 |
Rwork | 0.240 |
R-free | 0.28360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6oqy |
RMSD bond length | 0.003 |
RMSD bond angle | 0.508 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.600 | 2.340 |
High resolution limit [Å] | 2.260 | 2.260 |
Rmeas | 0.217 | 0.903 |
Rpim | 0.050 | |
Number of reflections | 12218 | 2148 |
<I/σ(I)> | 10.8 | |
Completeness [%] | 99.7 | |
Redundancy | 16.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291.15 | Na acetate (pH 4.6), PEG 4000, glycerol |