6VG6
Crystal structure of DPO4 with 8-oxoadenine (oxoA) and dGTP*
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2019-04-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.975, 97.761, 101.815 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.150 - 3.080 |
Rwork | 0.254 |
R-free | 0.30210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jx4 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.776 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.17.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.140 |
High resolution limit [Å] | 3.080 | 3.080 |
Rpim | 0.059 | 0.461 |
Number of reflections | 19085 | 1027 |
<I/σ(I)> | 10.2 | |
Completeness [%] | 98.6 | |
Redundancy | 3.3 | |
CC(1/2) | 0.486 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 16% PEG3350 50 mM Tris 100 mM Magnesium acetate |