6TC0
Crystal structure of MMS19-CIAO1-CIAO2B CIA targeting complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-06 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 107.400, 140.700, 327.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 3.600 |
R-factor | 0.2591 |
Rwork | 0.258 |
R-free | 0.27710 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.312 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 3.730 |
High resolution limit [Å] | 3.600 | 3.600 |
Number of reflections | 111722 | 11172 |
<I/σ(I)> | 12 | |
Completeness [%] | 98.4 | |
Redundancy | 41.4 | |
CC(1/2) | 1.000 | 0.124 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM HEPES pH 7.5, 25% PEG 3350 |