Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-07-05 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.999987 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 90.565, 90.565, 122.387 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.250 - 1.800 |
| Rwork | 0.182 |
| R-free | 0.20260 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5mut |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.365 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.293 | 1.840 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 54364 | 3192 |
| <I/σ(I)> | 17.6 | |
| Completeness [%] | 100.0 | |
| Redundancy | 9 | |
| CC(1/2) | 0.999 | 0.691 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 4.8 | 293 | 32% PEG 400 0.2M KSCN 0.2M NaBr 0.1M acetate 4.8 |
