6RPZ
Cytokine receptor-like factor 3 C-terminus residues 174-442: native collected with 1.7A wavelength
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-23 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.7007 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 87.800, 40.600, 76.660 |
Unit cell angles | 90.00, 99.80, 90.00 |
Refinement procedure
Resolution | 32.150 - 1.740 |
R-factor | 0.175 |
Rwork | 0.173 |
R-free | 0.20540 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 6rpx |
RMSD bond length | 0.011 |
RMSD bond angle | 1.080 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.150 | 1.790 |
High resolution limit [Å] | 1.740 | 1.740 |
Rmerge | 0.057 | 0.778 |
Rmeas | 0.064 | 0.913 |
Number of reflections | 24310 | 6424 |
<I/σ(I)> | 20 | 2.1 |
Completeness [%] | 88.4 | 49.2 |
Redundancy | 9.3 | 6.4 |
CC(1/2) | 0.999 | 0.492 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 12 % PEG 3,350, 0.1M sodium acetate . Cryoprotected in 25 % ethylene glycol |