6QMQ
NF-YB/C Heterodimer in Complex with NF-YA-derived Peptide Stabilized with C8-Hydrocarbon Linker
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-29 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.977930 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.010, 52.210, 72.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.890 - 2.500 |
R-factor | 0.1795 |
Rwork | 0.172 |
R-free | 0.24120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4csr |
RMSD bond length | 0.014 |
RMSD bond angle | 1.627 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 6325 | 682 |
<I/σ(I)> | 11.07 | 2.18 |
Completeness [%] | 99.6 | 100 |
Redundancy | 12.2 | 12.9 |
CC(1/2) | 0.997 | 0.665 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277.15 | 0.1 M sodium cacodylate pH6.5 0.2 M calcium acetate 37% PEG600 |