6OD4
Human TCF4 C-terminal bHLH domain in Complex with 11-bp Oligonucleotide Containing E-box Sequence
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-08-16 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 |
Unit cell lengths | 36.614, 43.602, 43.557 |
Unit cell angles | 97.17, 102.56, 102.53 |
Refinement procedure
Resolution | 41.817 - 1.699 |
R-factor | 0.2242 |
Rwork | 0.222 |
R-free | 0.26680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ql2 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.423 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.820 | 1.750 |
High resolution limit [Å] | 1.699 | 1.700 |
Rmerge | 0.103 | 0.711 |
Rpim | 0.041 | 0.418 |
Number of reflections | 26021 | 2269 |
<I/σ(I)> | 16.4 | 3.7 |
Completeness [%] | 95.3 | 83.1 |
Redundancy | 6.2 | 3.2 |
CC(1/2) | 0.522 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 292 | 20% PEG4000, 10% 2-propanol, 0.1 M sodium citrate tribasic dihydrate, pH 5.6 |