6O6P
Structure of the regulator FasR from Mycobacterium tuberculosis in complex with DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-02 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97948 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 61.697, 174.680, 158.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.066 - 3.851 |
R-factor | 0.2919 |
Rwork | 0.287 |
R-free | 0.33150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6o6n |
Data reduction software | TRUNCATE |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 39.540 | 39.540 | 4.310 |
High resolution limit [Å] | 3.850 | 8.610 | 3.850 |
Rmerge | 0.166 | 0.063 | 1.454 |
Rmeas | 0.176 | 0.066 | 1.581 |
Rpim | 0.055 | 0.020 | 0.595 |
Number of reflections | 6467 | 821 | 1452 |
<I/σ(I)> | 8.3 | ||
Completeness [%] | 76.5 | 99 | 62.3 |
Redundancy | 8.6 | 11 | 5.6 |
CC(1/2) | 0.997 | 0.998 | 0.623 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 28% PEG2000 MME, 0.25 M ammonium citrate, 0.1 M imidazole |