6MRG
FAAH bound to non covalent inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 273 |
| Detector technology | PIXEL |
| Collection date | 2011-10-22 |
| Detector | DECTRIS PILATUS3 R 1M |
| Wavelength(s) | 1.0094 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 144.208, 152.014, 299.914 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.392 - 2.770 |
| R-factor | 0.192 |
| Rwork | 0.195 |
| R-free | 0.24000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.319 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.392 | 2.910 |
| High resolution limit [Å] | 2.760 | 2.760 |
| Rmerge | 0.086 | 0.623 |
| Number of reflections | 78055 | 10777 |
| <I/σ(I)> | 12.35 | 2.58 |
| Completeness [%] | 92.2 | 88.7 |
| Redundancy | 4.7 | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.4 | 277 | PEG8000, PHOSPHATE, PH 7.4 |
