6M6F

Solution structure of disulfide bond mutaion of the core domain of Fibroblast growth factor 21 (FGF21)

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE III		600
2	Bruker	AVANCE III		850

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	1	2D 1H-15N HSQC
10	1	2	3D HN(CA)CO
11	1	2	3D 1H-13C NOESY
12	1	1	3D 1H-15N NOESY
13	1	3	3D HCCH-TOCSY
14	1	3	3D HCCH-COSY
15	1	3	3D 1H-13C NOESY
2	1	2	2D 1H-15N HSQC
3	1	3	2D 1H-15N HSQC
4	1	2	3D CBCA(CO)NH
5	1	2	3D HNCO
6	1	2	3D HNCA
7	1	2	3D HNCACB
8	1	2	3D HBHA(CO)NH
9	1	2	3D HN(CO)CA

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	7	1	298

Conformers

Conformers Calculated Total Number	200
Conformers Submitted Total Number	10