6LVL
Crystal structure of FGFR2 in complex with 1,3,5-triazine derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NE3A |
Synchrotron site | Photon Factory |
Beamline | AR-NE3A |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2009-12-24 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 105.675, 116.136, 64.202 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.110 - 2.980 |
R-factor | 0.2043 |
Rwork | 0.202 |
R-free | 0.25060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3b2t |
RMSD bond length | 0.005 |
RMSD bond angle | 1.658 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.040 |
High resolution limit [Å] | 2.980 | 8.110 | 2.990 |
Rmerge | 0.119 | 0.051 | 0.357 |
Number of reflections | 14661 | 705 | 758 |
<I/σ(I)> | 9.9 | ||
Completeness [%] | 87.7 | 75.5 | 91.3 |
Redundancy | 3.9 | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 296 | Tris, Ammonium sulfate, PEG 8000 |