6KRO
Tankyrase-2 in complex with RK-582
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-02-01 |
Detector | RAYONIX MX225-HS |
Wavelength(s) | 1.000 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 66.116, 66.116, 114.758 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.750 - 1.900 |
R-factor | 0.1733 |
Rwork | 0.172 |
R-free | 0.20310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.028 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.750 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmeas | 0.114 | 2.047 |
Rpim | 0.030 | 0.534 |
Number of reflections | 20832 | 1317 |
<I/σ(I)> | 16.3 | 1.6 |
Completeness [%] | 100.0 | |
Redundancy | 14.3 | |
CC(1/2) | 0.999 | 0.615 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | 0.1M Tris pH 8.5, 1.6M (NH4)2HPO4 |