6KNR

Crystal structure of Estrogen-related receptor gamma ligand-binding domain with DN200699

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-06-20
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.00003
Spacegroup name	P 43 21 2
Unit cell lengths	119.916, 119.916, 125.981
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.835 - 2.804
R-factor	0.1848
Rwork	0.183
R-free	0.22560
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1s9q
RMSD bond length	0.008
RMSD bond angle	0.985
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.15.2_3472: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.850
High resolution limit [Å]	2.800	2.800
Rmerge	0.079	0.149
Rmeas	0.082	0.154
Rpim	0.022	0.041
Number of reflections	23172	23172
<I/σ(I)>	45.2
Completeness [%]	100.0	100
Redundancy	13.5	14.2
CC(1/2)	0.998	0.994

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	0.28M K Na Tartrate