6J10
Ciclopirox inhibits Hepatitis B Virus secretion by blocking capsid assembly
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2018-03-21 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.97934 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 153.924, 88.510, 99.162 |
Unit cell angles | 90.00, 121.13, 90.00 |
Refinement procedure
Resolution | 30.700 - 2.300 |
R-factor | 0.25975 |
Rwork | 0.257 |
R-free | 0.30346 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.367 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.890 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 47285 | |
<I/σ(I)> | 30.1 | |
Completeness [%] | 98.0 | |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 100mM ammonium citrate pH 6.0, 14% PEG5000MME, 2% hexylene glycol, 10% isopropanol |