6IF3
Complex structure of Rab35 and its effector ACAP2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-27 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.741, 53.468, 144.008 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.530 |
High resolution limit [Å] | 1.500 | 4.070 | 1.500 |
Rmerge | 0.117 | 0.077 | 0.584 |
Rmeas | 0.122 | 0.080 | 0.636 |
Rpim | 0.035 | 0.023 | 0.239 |
Total number of observations | 570145 | ||
Number of reflections | 54675 | 3077 | 1913 |
<I/σ(I)> | 5.2 | ||
Completeness [%] | 96.7 | 99.9 | 68.8 |
Redundancy | 10.4 | 12.1 | 4.9 |
CC(1/2) | 0.997 | 0.801 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | Potassium sodium tartrate, PEG 3350 |