6GMR
pVHL:EloB:EloC in complex with (4-(1H-pyrrol-1-yl)phenyl)methanol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-06-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.07169 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 59.880, 59.880, 246.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.843 - 1.750 |
R-factor | 0.2122 |
Rwork | 0.211 |
R-free | 0.23550 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.844 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | BUSTER-TNT |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.850 |
High resolution limit [Å] | 1.750 | 1.750 |
Number of reflections | 45106 | |
<I/σ(I)> | 28.69 | 2.48 |
Completeness [%] | 96.5 | 99.2 |
Redundancy | 12.1 | 12.5 |
CC(1/2) | 1.000 | 0.865 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 290 | 0.1 M K phosphate pH 6.6, 0.2 M AS, 20% PEG MME 5000, 5% DTT |