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6FZH

Crystal structure of a streptococcal dehydrogenase at 1.5 Angstroem resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-2
Synchrotron siteESRF
BeamlineID23-2
Temperature [K]100
Detector technologyCCD
Collection date2012-05-16
DetectorADSC QUANTUM 315
Wavelength(s)0.87260
Spacegroup nameP 21 21 2
Unit cell lengths79.266, 91.603, 106.265
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution44.130 - 1.500
R-factor0.1487
Rwork0.148
R-free0.16280
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3lvf
RMSD bond length0.006
RMSD bond angle1.032
Data reduction softwareXDS (March 15, 2012)
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.1301.550
High resolution limit [Å]1.5001.500
Rmerge0.0600.493
Rmeas0.0710.642
Number of reflections12257410880
<I/σ(I)>15.811.66
Completeness [%]98.588.69
Redundancy3.52.1
CC(1/2)0.9970.527
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.42930.2 M potassium nitrate, 22% w/v PEG 3350

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