6FWX
Chimeric titin Z1Z2-Z1Z2 tandem (Z1212) functionalized with a GRGDS exogenous peptide from fibronectin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97400 |
Spacegroup name | H 3 |
Unit cell lengths | 134.400, 134.400, 134.000 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.798 - 3.000 |
R-factor | 0.2008 |
Rwork | 0.200 |
R-free | 0.22550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2a38 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.461 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.800 | 3.108 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 1.803 | |
Rmeas | 2.079 | |
Number of reflections | 17993 | 1813 |
<I/σ(I)> | 9.26 | 0.6 |
Completeness [%] | 99.0 | |
Redundancy | 4.1 | |
CC(1/2) | 0.162 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 10% [v/v] isopropanol, 100 mM Na2HPO4 pH 4.2, 200 mM LiSO4 |