6FUK
Crystal structure of UTX complexed with 5-carboxy-8-hydroxyquinoline
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-06 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.999998 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 80.417, 83.261, 92.898 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 46.449 - 2.000 |
| R-factor | 0.1884 |
| Rwork | 0.186 |
| R-free | 0.22830 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3avs |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.806 |
| Data reduction software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.449 | 5.950 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 42377 | 6776 |
| <I/σ(I)> | 12.58 | 1.67 |
| Completeness [%] | 98.3 | 98.4 |
| Redundancy | 3.7 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | 0.1 M Tris-HCl (pH 8.5), Li2 SO4 (0.15-0.25 M), PEG 3350 (20-25% w/v) |
