6FHT
Crystal structure of an artificial phytochrome regulated adenylate/guanylate cyclase in its dark adapted Pr form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-06 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0332 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 286.190, 108.820, 67.990 |
Unit cell angles | 90.00, 100.84, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.847 | 46.847 | 2.450 |
High resolution limit [Å] | 2.350 | 10.000 | 2.350 |
Rmerge | 0.089 | 0.037 | 0.983 |
Rmeas | 0.096 | 0.040 | 1.069 |
Number of reflections | 82012 | 1131 | 7967 |
<I/σ(I)> | 13.78 | 37.28 | 1.96 |
Completeness [%] | 96.1 | 96.8 | 80.1 |
Redundancy | 6.77 | 6.025 | 6.48 |
CC(1/2) | 0.998 | 0.999 | 0.672 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 0.1 M bis-Tris (pH 5.5), 1 M ammonium sulfate, 1 % (w/v) polyethylene glycol 3,350 |