6F8U
Crystal structure of the PDE4D catalytic domain in complex with GEBR-20b
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-06 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 64.672, 98.669, 119.644 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.334 - 2.100 |
R-factor | 0.1682 |
Rwork | 0.166 |
R-free | 0.21900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6f6u |
RMSD bond length | 0.008 |
RMSD bond angle | 0.990 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.348 | 2.614 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.068 | |
Number of reflections | 45081 | |
<I/σ(I)> | 16.5 | |
Completeness [%] | 99.8 | |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Hepes PEG 3350 Magnesium Chloride |