6F7C
TUBULIN-Compound 12 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-10 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00004 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.810, 157.900, 180.770 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.542 - 2.002 |
R-factor | 0.2133 |
Rwork | 0.212 |
R-free | 0.24310 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5lxt |
RMSD bond length | 0.006 |
RMSD bond angle | 0.773 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2863: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.105 | 3.984 |
Rmeas | 0.109 | 4.131 |
Number of reflections | 199860 | 14518 |
<I/σ(I)> | 17.81 | 0.73 |
Completeness [%] | 99.8 | 98.7 |
Redundancy | 13.5 | 13.2 |
CC(1/2) | 0.999 | 0.254 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.5 | 293 | 5% PEG 4K, 16% GLYCEROL, 30 MM MAGNESIUM CHLORIDE, 30 MM CALCIUM CHLORIDE, 0.1M MES/0.1M IMIDAZOLE |