6EOP

DPP8 - SLRFLYEG, space group 20

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-09-04
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.99992
Spacegroup name	C 2 2 21
Unit cell lengths	162.830, 246.371, 261.191
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.620 - 2.400
R-factor	0.21474
Rwork	0.214
R-free	0.23663
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1orv
RMSD bond length	0.006
RMSD bond angle	1.145
Data reduction software	XDS
Data scaling software	xia2
Phasing software	PHASER
Refinement software	REFMAC (5.8.0155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.620	2.560
High resolution limit [Å]	2.400	2.400
Number of reflections	203220	34229
<I/σ(I)>	22.8	2.09
Completeness [%]	100.0	99.8
Redundancy	8.44	8.4
CC(1/2)		0.719

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	Na citrate 0.46M