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6EKQ

Crystal structure of the human BRPF1 bromodomain complexed with BZ054 in space group C2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyPIXEL
Collection date2017-09-21
DetectorDECTRIS PILATUS3 2M
Wavelength(s)0.999989
Spacegroup nameC 1 2 1
Unit cell lengths71.208, 57.784, 70.446
Unit cell angles90.00, 108.66, 90.00
Refinement procedure
Resolution43.886 - 1.650
R-factor0.1584
Rwork0.157
R-free0.18160
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4lc2
RMSD bond length0.009
RMSD bond angle1.033
Data reduction softwareMantid
Data scaling softwareADDREF
Phasing softwareMOLREP
Refinement softwarePHENIX ((1.12_2829: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]43.8901.680
High resolution limit [Å]1.6501.650
Rmerge0.0460.345
Number of reflections326021588
<I/σ(I)>183.4
Completeness [%]99.7100
Redundancy4.64.2
CC(1/2)0.9990.879
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2770.1 M Bis-Tris Propane pH9, 10% EG, 0.15M NaNO3, 25% PEG3350

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