6EJ0

Crystal structure of KDM5B in complex with KDOPZ000049a.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-10
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.97950
Spacegroup name	P 65 2 2
Unit cell lengths	141.820, 141.820, 151.750
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	51.807 - 2.060
R-factor	0.1914
Rwork	0.190
R-free	0.21040
RMSD bond length	0.008
RMSD bond angle	0.979
Data reduction software	xia2
Data scaling software	xia2
Phasing software	MOLREP
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	64.240	2.110
High resolution limit [Å]	2.060	2.060
Rmerge	0.094	2.416
Number of reflections	56074	4074
<I/σ(I)>	21.6	1.4
Completeness [%]	100.0	100
Redundancy	19.8	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	277	0.1M HEPES pH 7.5, 0.8M Pottassium Phosphate-dibasic, 0.8M Sodium Phosphate monobasic