6EJ0
Crystal structure of KDM5B in complex with KDOPZ000049a.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-10 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97950 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 141.820, 141.820, 151.750 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 51.807 - 2.060 |
R-factor | 0.1914 |
Rwork | 0.190 |
R-free | 0.21040 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.979 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.240 | 2.110 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.094 | 2.416 |
Number of reflections | 56074 | 4074 |
<I/σ(I)> | 21.6 | 1.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 19.8 | 20 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 0.1M HEPES pH 7.5, 0.8M Pottassium Phosphate-dibasic, 0.8M Sodium Phosphate monobasic |