6EG8
Structure of the GDP-bound Gs heterotrimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2015-08-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.03320 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 100.860, 100.810, 179.330 |
Unit cell angles | 90.00, 106.18, 90.00 |
Refinement procedure
Resolution | 48.433 - 2.800 |
R-factor | 0.2182 |
Rwork | 0.217 |
R-free | 0.26940 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.493 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3228) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.440 | 2.870 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 85278 | |
<I/σ(I)> | 4.28 | |
Completeness [%] | 99.9 | |
Redundancy | 8.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 17.5%(w/v) PEG 3350, 0.1M MgCl2 |