6EG0
Crystal structure of Dpr4 Ig1-Ig2 in complex with DIP-Eta Ig1-Ig3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | .97918 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 94.294, 94.294, 212.463 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.987 - 2.900 |
R-factor | 0.2233 |
Rwork | 0.221 |
R-free | 0.26350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB entries 5EO9 4cmm & 5K6U |
RMSD bond length | 0.002 |
RMSD bond angle | 0.492 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.200 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.114 | 0.686 |
Number of reflections | 24914 | 3936 |
<I/σ(I)> | 9.7 | |
Completeness [%] | 99.5 | |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 28% Edo_p8k (Molecular Dimensions), 0.1 M Morpheus Buffer 2, pH 7.5 (Molecular Dimensions), 10% carboxylic acid (Molecular Dimensions) |