6E8E
Crystal structure of the Escherichia coli sliding clamp-MutL complex.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-06-06 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97951 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.390, 103.210, 141.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.830 | 2.320 |
High resolution limit [Å] | 2.070 | 2.250 |
Number of reflections | 53370 | |
<I/σ(I)> | 11.5 | |
Completeness [%] | 97.5 | |
Redundancy | 4.4 | |
CC(1/2) | 0.998 | 0.356 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 100 mM Bis-Tris pH 5.5, 2 M ammonium sulfate. |