Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

6DGU

PER-2 class A extended-spectrum beta-lactamase crystal structure at 2.69 Angstrom resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 2
Synchrotron siteSOLEIL
BeamlinePROXIMA 2
Temperature [K]100
Detector technologyPIXEL
Collection date2016-12-11
DetectorDECTRIS EIGER X 9M
Wavelength(s)0.980100
Spacegroup nameP 21 21 21
Unit cell lengths82.370, 82.580, 174.920
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution41.290 - 2.691
R-factor0.2713
Rwork0.267
R-free0.33960
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4d2o
RMSD bond length0.010
RMSD bond angle1.357
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHENIX (1.12-2829)
Refinement softwarePHENIX (1.12_2829)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]41.2902.850
High resolution limit [Å]2.6912.691
Rmerge0.1640.450
Rmeas0.1800.500
Number of reflections329514944
<I/σ(I)>9.743.63
Completeness [%]97.391.4
Redundancy5.465.46
CC(1/2)0.9870.780
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP29420% PEG 6000, 0.05 M imidazole pH=8.0

217705

PDB entries from 2024-03-27

PDB statisticsPDBj update infoContact PDBjnumon