6BW5
Human GPT (DPAGT1) in complex with tunicamycin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 212.272, 105.512, 149.389 |
Unit cell angles | 90.00, 103.53, 90.00 |
Refinement procedure
Resolution | 83.048 - 3.100 |
R-factor | 0.2577 |
Rwork | 0.256 |
R-free | 0.28840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5lev |
RMSD bond length | 0.003 |
RMSD bond angle | 0.672 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.211 |
High resolution limit [Å] | 3.100 | 3.100 |
Rpim | 0.068 | |
Number of reflections | 35101 | 5815 |
<I/σ(I)> | 13.65 | |
Completeness [%] | 97.5 | 96.29 |
Redundancy | 79.9 | 69.1 |
CC(1/2) | 0.963 | 0.592 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 290 | PEG400, calcium chloride |