6BT0
CRYSTAL STRUCTURE OF RHEB IN COMPLEX WITH COMPOUND NR1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2016-04-11 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 |
Unit cell lengths | 49.150, 60.140, 66.320 |
Unit cell angles | 68.35, 90.01, 72.05 |
Refinement procedure
Resolution | 46.370 - 2.600 |
R-factor | 0.2219 |
Rwork | 0.217 |
R-free | 0.31640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1xtq |
RMSD bond length | 0.012 |
RMSD bond angle | 1.619 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0103) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.370 | 46.370 | 1.830 |
High resolution limit [Å] | 1.780 | 7.960 | 1.780 |
Rmerge | 0.312 | 0.031 | |
Rmeas | 0.441 | 0.043 | |
Number of reflections | 18856 | 690 | 2735 |
<I/σ(I)> | 2.58 | 19.59 | 0.03 |
Completeness [%] | 84.7 | 96.1 | 57.9 |
Redundancy | 1.989 | 1.986 | 1.958 |
CC(1/2) | 0.959 | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 19% PEG 1500, 0.1M Na acetate pH 5.0 |