6BDZ
ADAM10 Extracellular Domain Bound by the 11G2 Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-04-15 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 79.230, 97.580, 262.720 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.790 - 3.100 |
R-factor | 0.2669 |
Rwork | 0.261 |
R-free | 0.31730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 0.693 |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.200 |
High resolution limit [Å] | 3.100 | 3.100 |
Number of reflections | 35539 | 1850 |
<I/σ(I)> | 4.05 | 0.87 |
Completeness [%] | 99.8 | 98.76 |
Redundancy | 10.6 | 10.5 |
CC(1/2) | 0.989 | 0.355 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 295 | 2.23M Ammonium Sulfate 100mM Tris pH 8.5 2% PEG400 |